Fabrication and characterization of nanoparticle MgO/B4C composite by mechanochemical method

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dc.contributor.authorGokmese, Hakan
dc.contributor.authorBostan, Bulent
dc.date.accessioned2024-02-23T14:26:58Z
dc.date.available2024-02-23T14:26:58Z
dc.date.issued2017
dc.departmentNEÜen_US
dc.description.abstractIn this study, nanoparticle boron carbide was produced after the reduction of boron oxide with magnesium under the presence of carbon by using mechanochemical synthesis method. During the synthesis processing, microstructure and phase transformations of powders were performed by using X-ray diffraction (XRD), Fourier-transform infrared spectrum (FT-IR), scanning electron microscope (SEM), and high-resolution transmission electron microscopy (HRTEM). At the end of 2h, reaction products (MgO, B4C) were determined by XRD and FT-IR examinations. Nanoparticle B4C single-phase crystalline structure from the MgO/B4C composite powder mixture, which was the reaction product, was obtained by leaching process. With the increase in the synthesis period, starting material peaks diminished and Fe peak intensity became evident. After the HRTEM examinations, it was determined that synthesized B4C particles were within range of 10-200 nm especially in the activation of leaching process. Additionally, by using spot pattern analysis method, planes represented by B4C particles were calculated.en_US
dc.identifier.doi10.1177/0954408916629106
dc.identifier.endpage694en_US
dc.identifier.issn0954-4089
dc.identifier.issn2041-3009
dc.identifier.issue4en_US
dc.identifier.scopus2-s2.0-85026250943en_US
dc.identifier.scopusqualityQ3en_US
dc.identifier.startpage684en_US
dc.identifier.urihttps://doi.org/10.1177/0954408916629106
dc.identifier.urihttps://hdl.handle.net/20.500.12452/14400
dc.identifier.volume231en_US
dc.identifier.wosWOS:000406532800007en_US
dc.identifier.wosqualityQ3en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSage Publications Ltden_US
dc.relation.ispartofProceedings Of The Institution Of Mechanical Engineers Part E-Journal Of Process Mechanical Engineeringen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectMechanochemical Synthesisen_US
dc.subjectNanocompositeen_US
dc.subjectBoron Carbideen_US
dc.titleFabrication and characterization of nanoparticle MgO/B4C composite by mechanochemical methoden_US
dc.typeArticleen_US

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