The synthesis of a novel DDPHC diazonium salt: Investigation of its usability in the determination of phenol and chlorophenols using CV, SWV and DPV techniques

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dc.contributor.authorCelik, Haci Hasan
dc.contributor.authorOzcan, Saniye
dc.contributor.authorMulazimoglu, Aysen Demir
dc.contributor.authorYilmaz, Ecir
dc.contributor.authorMercimek, Bedrettin
dc.contributor.authorCukurovali, Alaaddin
dc.contributor.authorYilmaz, Ibrahim
dc.date.accessioned2024-02-23T14:03:16Z
dc.date.available2024-02-23T14:03:16Z
dc.date.issued2020
dc.departmentNEÜen_US
dc.description.abstractElectrochemical and spectroelectrochemical properties of newly synthesized diazonium salt of 2-(2-(1,3-dioxo- 3,3a-dihydro-1H-isoindol-2(7aH)-yl)-1-(3 methyl-3-phenylcyclobutyl)ethylidene) hydrazinecarboxamide (DDPHC-DAS) were studied using glassy carbon (GC) electrode. In the current study, surface characterization was performed by cyclic voltammetry (CV). Besides electrochemical impedance spectroscopy (EIS) was used for the electrochemical and spectroelectrochemical characterization. Surface images were obtained using scanning electron microscopy (SEM). After completion of modification and characterization process, DDPHC-DAS surface was examined for the usability for the quantitative determination of phenol and chlorophenol derivatives by using CV, square wave voltammetry (SWV) and differential pulse voltammetry (DPV). Phenol and chlorophenol solutions that were prepared in Britton-Robinson (BR) buffer solution (pH 8-12) were employed in this research. The presented study proves that all of compounds can be quantitatively determined not only simultaneously but also independently.en_US
dc.description.sponsorshipResearch Foundation of Necmettin Erbakan University, Konya-TURKEY [BAP-131210012, 161410005]en_US
dc.description.sponsorshipWe would like to thank to the Research Foundation of Necmettin Erbakan University, Konya-TURKEY (BAP-131210012 and 161410005) for financial support of this work.en_US
dc.identifier.doi10.1016/j.inoche.2020.107893
dc.identifier.issn1387-7003
dc.identifier.issn1879-0259
dc.identifier.scopus2-s2.0-85082180286en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.urihttps://doi.org/10.1016/j.inoche.2020.107893
dc.identifier.urihttps://hdl.handle.net/20.500.12452/12043
dc.identifier.volume116en_US
dc.identifier.wosWOS:000530085000002en_US
dc.identifier.wosqualityQ2en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherElsevieren_US
dc.relation.ispartofInorganic Chemistry Communicationsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectDdphg-Dasen_US
dc.subjectCyclic Voltammetryen_US
dc.subjectSquare Wave Voltammetryen_US
dc.subjectDifferential Pulse Voltammetryen_US
dc.subjectChemical Sensor Electrodeen_US
dc.titleThe synthesis of a novel DDPHC diazonium salt: Investigation of its usability in the determination of phenol and chlorophenols using CV, SWV and DPV techniquesen_US
dc.typeArticleen_US

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