Borik asit katkılı elektro porselen üretimi ve özelliklerinin incelenmesi
Yükleniyor...
Tarih
2015
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
Sanayinin gelişmesi elektrik enerjisine ihtiyacı artırarak, izolatörlerin dış etkenlere ve artan şebeke voltajına karşı teknik özelliklerinin, mekanik dayanımının arttırılmasını ve ucuz yollu izolatör üretiminin gerekliliğini ortaya koymuştur. Bu amaçla, elektro-porselen masse çamuruna, 0,1, 0,3 ve 1 H3BO3 katkılı hazırlanan numuneler, vakum preste şekillendirilerek kurutulduktan sonra, 1255 oC sıcaklıkta, 2 saatte ve hava atmosferinde sinterlenmiştir. Numunelere tane boyut dağılımı, kuru küçülme, fuksin ve üç nokta eğme testleri uygulanmıştır. Mikroyapı karakterizasyonları bakımından XRD, SEM ve EDS analizleri yapılmıştır. 0,3e kadar borik asit katkılı numunede tane boyut dağılımında azalma, 1 katkılı numunede kuru küçülme miktarında azalmanın en fazla ve genel olarak 0,3 borik asit katkılı numunenin işletme değerlerine daha yakın sonuçlar verdiği tespit edilmiştir. Dolayısıyla borik asit, elektro porselen bünyesine katkı maddesi olarak belirli oranda katılabildiğinde alternatif bir hammadde kaynağı olabileceği gözlemlenmiştir.
The need of electrical energy is raised by the development of industry and that required to transportation of energy to the more distant points. All these developments reveal the need of cheaper insulator production and the need of enhancement of insulators’ technical specifications and mechanical resistance against the increasing mains voltage and external factors. In the study, three different prescriptions, contain 0.1 , 0.3 and 1 H3BO3 additive, were prepared. Then, prepared samples were shaped on vacuum presses in the laboratory. After samples were dried, they were sintered at 1255 ºC for 2 hours in air. Particle size distribution, dry refinement, fuchsine and bending three point tests were applied to the samples. Characterizations of microstructure were performed by XRD, SEM and EDS analyses. At the end of the experimental studies, it was seen that depending on additive percentage, the reduction of particle size distribution is up to 0.3 and particle size is increasing with an increase in additive ratio. The maximum dry reduction amount was seen on the sample that contains 1 boric acid. In general, it was determined that the sample, which contains 0.3 boric acid, gives closer results to operation conditions. Therefore, it was observed that the boric acid could be an alternative raw material source, if it is incorporate into electro-ceramic at a certain ratio.
The need of electrical energy is raised by the development of industry and that required to transportation of energy to the more distant points. All these developments reveal the need of cheaper insulator production and the need of enhancement of insulators’ technical specifications and mechanical resistance against the increasing mains voltage and external factors. In the study, three different prescriptions, contain 0.1 , 0.3 and 1 H3BO3 additive, were prepared. Then, prepared samples were shaped on vacuum presses in the laboratory. After samples were dried, they were sintered at 1255 ºC for 2 hours in air. Particle size distribution, dry refinement, fuchsine and bending three point tests were applied to the samples. Characterizations of microstructure were performed by XRD, SEM and EDS analyses. At the end of the experimental studies, it was seen that depending on additive percentage, the reduction of particle size distribution is up to 0.3 and particle size is increasing with an increase in additive ratio. The maximum dry reduction amount was seen on the sample that contains 1 boric acid. In general, it was determined that the sample, which contains 0.3 boric acid, gives closer results to operation conditions. Therefore, it was observed that the boric acid could be an alternative raw material source, if it is incorporate into electro-ceramic at a certain ratio.
Açıklama
Anahtar Kelimeler
Electro porcelain, Boric acid, Sintering, Elektro porselen, Borik asit, Sinterleme
Kaynak
Gazi Üniversitesi Mühendislik Mimarlık Fakültesi Dergisi
WoS Q Değeri
Scopus Q Değeri
Q2
Cilt
30
Sayı
4
Künye
Gökmeşe, H., Bilgin, A. E., Bostan, B. (2015). Borik asit katkılı elektro porselen üretimi ve özelliklerinin incelenmesi. Gazi Üniversitesi Mühendislik Mimarlık Fakültesi Dergisi, 30, 4, 577-583.
