Characterization of W2B nanocrystals synthesized by mechanochemical method
Yükleniyor...
Tarih
2016
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Erişim Hakkı
info:eu-repo/semantics/openAccess
Özet
In this study; W2B nanocrystals were synthesized with B2 O3 /Mg/WO3 starting materials via mechanochemical method. Starting materials were mixed according to the reaction stoichiometry and reduction processes were performed in a planetary ball mill under Argon gas atmosphere. Phase and morphology structure of particles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy with energy-dispersive X-ray spectroscopy (TEM/EDX) and the specific surface area was measured by Brunauer-Emmet-Teller (BET) theory. The effect of milling period and molar ratios of starting powders were investigated in detail. Results showed that W2 B nanocrystals were obtained successfully without different tungsten compounds after 30 h milling and purification in 2 M HCl solution. Coaxial/spherical shaped and agglomerated W2 B nanocrystals were observed by microstructural examinations. Crystallite size and specific surface area of the W2 B nanocrystals were determined as 13.61 nm and 18 m2 /g respectively.
Açıklama
Anahtar Kelimeler
Ball milling, Mechanochemical synthesis, Nanocrystals, W2B
Kaynak
Bor Dergisi
WoS Q Değeri
Scopus Q Değeri
Cilt
1
Sayı
1
Künye
Barış, M., Şimşek, T., Gökmeşe, H., Akkurt, A. (2016). Characterization of W2B nanocrystals synthesized by mechanochemical method. Bor Dergisi, 1, 1, 45-51.
