Characterization of W2B nanocrystals synthesized by mechanochemical method

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dc.authoridHakan Gökmeşe: 0000-0003-0053-8444
dc.authoridTuncay Şimşek: 0000-0002-4683-0152
dc.authoridAdnan Akkurt: 0000-0002-0622-1352
dc.contributor.authorBarış, Mustafa
dc.contributor.authorŞimşek, Tuncay
dc.contributor.authorGökmeşe, Hakan
dc.contributor.authorAkkurt, Adnan
dc.date.accessioned2020-01-18T21:02:55Z
dc.date.available2020-01-18T21:02:55Z
dc.date.issued2016
dc.departmentNEÜ, Seydişehir Ahmet Cengiz Mühendislik Fakültesi, Makine Mühendisliği Bölümüen_US
dc.description.abstractIn this study; W2B nanocrystals were synthesized with B2 O3 /Mg/WO3 starting materials via mechanochemical method. Starting materials were mixed according to the reaction stoichiometry and reduction processes were performed in a planetary ball mill under Argon gas atmosphere. Phase and morphology structure of particles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy with energy-dispersive X-ray spectroscopy (TEM/EDX) and the specific surface area was measured by Brunauer-Emmet-Teller (BET) theory. The effect of milling period and molar ratios of starting powders were investigated in detail. Results showed that W2 B nanocrystals were obtained successfully without different tungsten compounds after 30 h milling and purification in 2 M HCl solution. Coaxial/spherical shaped and agglomerated W2 B nanocrystals were observed by microstructural examinations. Crystallite size and specific surface area of the W2 B nanocrystals were determined as 13.61 nm and 18 m2 /g respectively.en_US
dc.identifier.citationBarış, M., Şimşek, T., Gökmeşe, H., Akkurt, A. (2016). Characterization of W2B nanocrystals synthesized by mechanochemical method. Bor Dergisi, 1, 1, 45-51.
dc.identifier.endpage51en_US
dc.identifier.issn2149-9020en_US
dc.identifier.issn2667-8438en_US
dc.identifier.issue1en_US
dc.identifier.startpage45en_US
dc.identifier.urihttps://app.trdizin.gov.tr/makale/TWpVME5ETTRPQT09/characterization-of-w2b-nanocrystals-synthesized-by-mechanochemical-method
dc.identifier.urihttps://hdl.handle.net/20.500.12452/1366
dc.identifier.volume1en_US
dc.indekslendigikaynakTR-Dizinen_US
dc.language.isoenen_US
dc.relation.ispartofBor Dergisien_US
dc.relation.publicationcategoryMakale - Ulusal Hakemli Dergi - Kurum Öğretim Elemanıen_US]
dc.rightsinfo:eu-repo/semantics/openAccessen_US
dc.subjectBall millingen_US
dc.subjectMechanochemical synthesisen_US
dc.subjectNanocrystalsen_US
dc.subjectW2Ben_US
dc.titleCharacterization of W2B nanocrystals synthesized by mechanochemical methoden_US
dc.typeArticleen_US

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